Effects of the continuous cooling process conditions on the crystallization and liberation characteristics of anosovite in Ti-bearing titanomagnetite smelting slag

Effects of the continuous cooling process conditions on the crystallization and liberation characteristics of anosovite in Ti-bearing titanomagnetite smelting slag

论文摘要

This study involved the investigation of the effects of the continuous cooling process conditions on the crystallization and liberation characteristics of anosovite in Ti-bearing titanomagnetite smelting slag. The samples were heated until melting and then the temperature was held at 1650℃ for nearly 0.5 h; subsequently, the samples were cooled at different cooling rates to different temperatures and water-quenched after being held for different times at these temperatures. Last, the obtained crystallized samples were used to analyze the crystallization and liberation characteristics. It was found that, during the continuous cooling process, anosovite particles were found to initially precipitate in the slag at a relatively high crystallization temperature, showing the characteristics of euhedral crystal. The precipitation and growth of anosovite grain is strong and the morphology of anosovite was basically not affected by the continuous cooling conditions. From the morphology perspective, the formed anosovite is an excellent Ti-rich phase to be selective separated. The formation of spinel and diopside is negative for the liberation and selective separation of the anosovite phase. The crystallization diagrams of TiO2-MgO-CaO-SiO2-Al2O3-FeO slag undergoing different continuous cooling processes were constructed to help to determine the optimal continuous cooling–quenching condition for selective separation of anosovite. Moreover, the addition of B2O3 can enlarge the range of the optimal continuous cooling–quenching conditions for selective separation of anosovite.

论文目录

  • 1. Introduction
  • 2. Experimental
  •   2.1. Sample preparation
  •   2.2. Experimental procedure
  •   2.3. Characterization
  • 3. Results and discussion
  •   3.1. Crystallization behavior
  •   3.2. Liberation characteristics
  • 4. Conclusions
  • 文章来源

    类型: 期刊论文

    作者: Zhen Wang,Hao-yan Sun,Qing-shan Zhu

    来源: International Journal of Minerals Metallurgy and Materials 2019年09期

    年度: 2019

    分类: 工程科技Ⅰ辑

    专业: 冶金工业

    单位: State Key Laboratory of Multiphase Complex Systems, Institute of Process Engineering, Chinese Academy of Sciences,School of Chemical Engineering, University of Chinese Academy of Sciences

    基金: financially supported by the National Natural Science Foundation of China (Nos. 51404226 and 21736010)

    分类号: TF823

    页码: 1120-1128

    总页数: 9

    文件大小: 535K

    下载量: 13

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    Effects of the continuous cooling process conditions on the crystallization and liberation characteristics of anosovite in Ti-bearing titanomagnetite smelting slag
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